Autors: Dimitrova, V. K.
Title: MICROSTRUCTURAL EVOLUTION AND MECHANICAL PROPERTIES OF COLD-DRAWN 1566 STEEL WIRE SUBJECTED TO HEAT TREATMENT RECRYSTALLIZATION ANNEALING
Keywords: AISI 1566 steel, Cold drawing, Grain growth, Holding time, Mechanical properties, Microstructure, Plasticity, Recrystallization annealing, Relative elongation, Temperature, Ultimate tensile strength

Abstract: Licensee IJOMAM, Romania.This study investigates the effects of recrystallization annealing on the mechanical properties and microstructure of cold-drawn AISI 1566 steel wire. Cold drawing is a highly precise metalworking process that enhances material properties such as mechanical strength, dimensional accuracy, and surface quality. The process induces significant dislocation accumulation, which, in combination with deformation mechanisms such as slip and formation of crystallographic twins at the nanoscale, optimizes material performance. The paper examines the temperature-dependent changes in hardness and microstructure, alongside the impact of recrystallization annealing on ultimate tensile strength (Rm) and relative elongation (δ). The results indicate that recrystallization annealing at temperatures ranging from 350°C to 730°C facilitates the formation of new, defect-free grains, thereby reducing internal stresses and improving plasticity. However, higher temperatures and extended holding times promote grain growth, leading to a reduction in mechanical strength while enhancing ductility. The study further explores the interplay between annealing temperature, holding time, and mechanical properties, emphasizing the importance of precise control over these parameters to achieve an optimal balance between strength and plasticity.

References

  1. Masoumi, M., Oliveira, S., Paredes, M. (2024). Influence of Cold Drawing on Phase Transformation and Tensile Properties of FeCrMn Austenitic Stainless Steel 201. Steel Research International, http://dx.doi.org/10.1002/srin.202400469.
  2. Yan, F., Ma, C., Jiang, J. Q., Feng, H.P., Zha, S.T. (2008). Effect of Cumulative Strain on Texture Characteristics during Wire Drawing of Eutectoid Steels. Scripta Materialia, Vol. 59, No. 8, Pp. 850-853. 2008. doi: http://dx.doi.org/10.1016/j.scriptamat.2008.06.048
  3. Humphreys, F., Hatherly, M. (2004). Recrystallization and Related Annealing Phenomena. 2nd Edition, Elsevier Ltd. Pergamon, Amsterdam, Pp. 658, 2004.
  4. Ferry, М. Influence of Fine Particle of Grain Coarsening within an Orientation Gradient. Acta Materialia, Vol. 53, No. 3, Pp. 773-783. 2005. doi: http://dx.doi.org/10.1016/j.actamat.2004.10.030
  5. Nurudeen, Р., Oluwole, L. (2013). Recrystallization Kinetics And Microstructure Evolution Of Annealed Cold-Drawn Low-Carbon Steel. Journal of Crystallization Process and Technology. Vol. 3, No. 4, Pp. 163-169. 2013. doi: http://dx.doi.org/10.4236/jcpt.2013.34025.
  6. Toribio, J. (2017). Structural integrity of progressively cold-drawn pearlitic steels: From Raffaello Sanzio to Vincent van Gogh. Procedia Structural Integrity. Procedia Structural Integrity. Vol. 3, No. 4, Pp. 3-10. doi: http://dx.doi.org/10.1016/j.prostr.2017.04.002.
  7. Li, X., Ma, B., Wang, C. (2025). Microstructure Evolution and Strengthening Mechanism of Regenerated Brass Alloy under Fe-Mn Control during Cold Drawing. Met. Mater. Int. Vol. 31, Pp. 595–612. 2025. doi: https://doi.org/10.1007/s12540-024-01754-1
  8. Heedong, D., Kim, Y., Mawardi, F., Listyawan, T.A., Baek, E.R., Park, N. (2021). The effect of cold drawing process on the microstructure evolution of Ti-4.5Al-2.5Fe-0.15O titanium alloy, Materials Letters, Vol. 286. 129219. 2021. doi: https://doi.org/10.1016/j.matlet.2020.129219
  9. Churaev, N.V. (2004), Surface forces and physicochemistry of surface pehnomena. Russian Chem. Reviews, Vol. 73:1. Pp. 25–36. 2004. doi: https://doi.org/10.1070/RC2004v073n01ABEH000867
  10. Deryagin, B.. (1992). Summary of development of the theory of stability of colloids and thin films. Russian Chemical Bulletin. Vol. 41. Pp. 1321-1328. doi: 10.1007/BF00864326.
  11. McMahon, C. J., Graham, C.D. (2013). Introduction to Engineering Materials: The Bicycle & the Walkman. Merion Books. Pp. 386. 1992
  12. Humphreys, F. J., Hatherly. M. (2012). Recrystallization and related annealing phenomena. Elsevier, 2012. doi: https://doi.org/10.1016/B978-0-08-044164-1.X5000-2
  13. Sakai, T., Belyakov, A., Kaibyshev, R., Miura, H., Jonas, J. Dynamic and post-dynamic recrystallization under hot, cold and severe plastic deformation conditions, Progress in Materials Science, Vol. 60. Pp. 130-207.2014. doi: https://doi.org/10.1016/j.pmatsci.2013.09.002.
  14. https://www.tec-science.com/material-science/heat-treatment-steel/annealing-process-of-steel-recrystallization-annealing. accessed on:07.03.2025
  15. Jiajie, L., Chen, J., You, Z., Deng, L., Wang, C., Chen, J., Xiao, L., Wang, B. (2024). Effect of annealing temperature on the evolution of microstructure, texture, and mechanical properties of hot-rolled 12Cr-ODS steel. Journal of Materials Research and Technology. Vol. 30. Pp. 4800-4812. 2024. doi: https://doi.org/10.1016/j.jmrt.2024.04.204.
  16. Dutta S., Panda, A., Mitra, A., Chatterjee, S., Roy, R. (2020). Microstructural evolution, recovery and recrystallization kinetics of isothermally annealed ultra low carbon steel, Materials Research Express, Vol. 7. 2020. doi: https://doi.org/10.1088/2053-1591/ab657c
  17. Ma, G.; Sheng, J.; Gao, Y.; Tuo, L.; Li, Y.; La, P. (2024). Effect of Annealing Temperature on Microstructure and Mechanical Properties of 00Cr21CuTi Stainless Steel Cold-Rolled Sheets. Metals. Vol. 14. 2024. doi: https://doi.org/10.3390/met14121367
  18. Tang, X., Cheng, G., Liu, Y., Wang, C., Meng, Z., Wang, Y., Liu, Zhang, Z., Huang, J., Yu, X., Xu, X. (2023). Microstructure and properties evolution during annealing in low-carbon Nb containing steel with high strength and electrical conductivity: an experimental and theoretical study. Journal of Materials Research and Technology. Vol. 27, Pp.3054-3066. 2023 doi: https://doi.org/10.1016/j.jmrt.2023.10.093.
  19. Sun, J., Shengwu, G., Shengdun, Z., Mingyue, M., You-Ning, L. (2020). Improving strength of cold-drawn wire by martensitic transformation in a 0.65 wt% C low-alloy steel. Materials Science and Engineering: A. Vol. 790. 2020. doi: https://doi.org/10.1016/j.msea.2020.139719
  20. Petrov, A., Scherbakov, A. (2023). Heat treatment effect of 65G and 60C2A steels on strength characteristics of the hydrodynamic oscillator built-in drill head." E3S Web of Conferences. Vol. 389. EDP Sciences, 2023.
  21. Berdiyev, D., Yusupov, A. (2020). Improving the Wear Resistance of Gear Teeth by Cyclic Quenching with Inductive Heating. Russian Engineering Research. Vol.40. Pp. 473-475. 2020. doi: https://doi.org/10.3103/S1068798X20060064.
  22. Kristoffersen M, Casadei F, Borvik T, Langseth M, Hopperstad O. (2014). Impact against empty and water-filled X65 steel pipes-Experiments and simulations. International journal of impact engineering. Vol. 71 Pp. 73-88. 2014. doi: https://doi.org/10.1016/j.ijimpeng.2014.04.004
  23. Gruben, G., Fagerholt, E., Hopperstad, O., Børvik, T. (2011). Fracture characteristics of a cold-rolled dual-phase steel, European Journal of Mechanics-A/Solids. Vol. 30. Issue 3. Pp. 204-218. 2011, doi: https://doi.org/10.1016/j.euromechsol.2011.01.004
  24. Novikov, V.F., Kulak, S.M., Muratov, K.R., Parakhin, A.S. (2022). Relationship between Magnetoelastic Sensitivity of Magnetoelastic Demagnetization of Steels 60G and 65G and Coercive Force and Magnetostriction. Russ. J. Nondestruct. Test. Vol. 58. Pp. 479–487. 2022, doi: https://doi.org/10.1134/s1061830922060079.
  25. https://songshunsteel.com/product/gb-65mn-steel-coil-aisi-1066-astm-1566/#mechanical. accessed on: 07.03.2025
  26. Ivanytskyi, Y., Тарас L., Molkov, Y., Kulyk, V., Duriagina, Z. (2016). Influence of 65G steel microstructure on crack faces friction factor under mode II fatigue fracture. Archives of Materials Science and Engineering. Vol. 82. Pp. 49-56. 2016. doi: https://doi.org/10.5604/01.3001.0009.7103.
  27. Sagdoldina, Z., Tyurin, Y., Berdimuratov, N., Stepanova, O., Magazov, N., Baizhan. D. (2023). Electrofrictional Hardening of the 40Kh and 65G Steels. Coatings. Vol. 13:11. Pp. 1820. doi: https://doi.org/10.3390/coatings13111820
  28. Nguyen, T., Tuan, Tr., Toan. V. (2024). A Case Study of Surface Roughness Improvement for C40 Carbon Steel and 201 Stainless Steel using Ultrasonic Assisted Vibration in Cutting Speed Direction. Engineering, Technology & Applied Science Research. Vol. 14. Pp. 15068-15073. 2024. doi: https://doi.org/10.48084/etasr.7552
  29. Vorobev R., Dubinskii, V. (2015). Comparison of the influence of heat treatment and magnetic-pulse treatment on the mechanical characteristics of 65G steel upon instrumental indentation, The Physics of Metals and Metallography, Vol. 116:11, Pp. 1159–1164. 2015 doi: https://doi.org/10.1134/S0031918X15110125
  30. Ivanytskyi, Y., Molkov, Y., Kun, P., Тарас L., Wójtowicz, M.. (2015). Determination of the Local Strains Near Stress Concentrators by the Digital Image Correlation Technique. Materials Science. Vol.50. Pp.488-495. 2015. doi: https://doi.org 10.1007/s11003-015-9746-7.
  31. Rakhadilov, B., Zhurerova, L., Pavlov, A. (2016). Method of Electrolyte-Plasma Surface Hardening of 65G and 20GL Low-Alloy Steels Samples. IOP Conference Series: Materials Science and Engineering. 142. doi; https://doi.org/10.1088/1757-899X/142/1/012028
  32. Liu, Y., Gan, X., Liang, W., Xu, G., Qi, J., Liu, M. (2023). Microstructure Evolution and Mechanical Response of a Direct Quenched and Partitioned Steel at Different Finishing Rolling Temperatures. Materials. Vol. 16. doi: https://doi.org/10.3390/ma16093575
  33. Zhang, P., Wang, D., Cheng, P., Shao, C., Zhu, W., Zhou, J., Jihua, H. (2022). Microstructure, mechanical properties and corrosion behaviour of 65Mn tape-steel via electromagnetic induction heating. Materials Today Communications. Vol. 30. 2022. doi: https://doi.org/10.1016/j.mtcomm.2022.103175

Issue

International Journal of Mechatronics and Applied Mechanics, vol. 1, pp. 95-102, 2025, Albania, https://doi.org/10.17683/ijomam/issue20.9

Вид: статия в списание, публикация в реферирано издание, индексирана в Scopus